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Richard K Marcus

TitleProfessor
InstitutionClemson University
DepartmentDepartment of Chemistry
Address223 Hunter Hall
Clemson, South Carolina 29634
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    1. Hoegg ED, Godin S, Szpunar J, Lobinski R, Koppenaal DW, Marcus RK. Ultra-High Resolution Elemental/Isotopic Mass Spectrometry (m/?m?>?1,000,000): Coupling of the Liquid Sampling-Atmospheric Pressure Glow Discharge with an Orbitrap Mass Spectrometer for Applications in Biological Chemistry and Environmental Analysis. J Am Soc Mass Spectrom. 2019 Apr 18. PMID: 31001752.
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    2. Trang HK, Jiang L, Marcus RK. Grafting polymerization of glycidyl methacrylate onto capillary-channeled polymer (C-CP) fibers as a ligand binding platform: Applications in immobilized metal-ion affinity chromatography (IMAC) protein separations. J Chromatogr B Analyt Technol Biomed Life Sci. 2019 Mar 15; 1110-1111:144-154. PMID: 30807967.
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    3. Bruce TF, Slonecki TJ, Wang L, Huang S, Powell RR, Marcus RK. Exosome isolation and purification via hydrophobic interaction chromatography using a polyester, capillary-channeled polymer fiber phase. Electrophoresis. 2019 Feb; 40(4):571-581. PMID: 30548636.
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    4. Wang L, Marcus RK. Evaluation of protein separations based on hydrophobic interaction chromatography using polyethylene terephthalate capillary-channeled polymer (C-CP) fiber phases. J Chromatogr A. 2019 Jan 25; 1585:161-171. PMID: 30502918.
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    5. Hoegg ED, Manard BT, Wylie EM, Mathew KJ, Ottenfeld CF, Marcus RK. Initial Benchmarking of the Liquid Sampling-Atmospheric Pressure Glow Discharge-Orbitrap System Against Traditional Atomic Mass Spectrometry Techniques for Nuclear Applications. J Am Soc Mass Spectrom. 2019 Feb; 30(2):278-288. PMID: 30291556.
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    6. Wang L, Marcus RK. Overload Effects in Reversed Phase Protein Separations using Capillary-Channeled Polymer Fiber Columns. Biotechnol Prog. 2018 09; 34(5):1221-1233. PMID: 30009535.
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    7. Paing HW, Marcus RK. Investigation of hydrophobic substrates for solution residue analysis utilizing an ambient desorption liquid sampling-atmospheric pressure glow discharge microplasma. Analyst. 2018 Mar 12; 143(6):1417-1425. PMID: 29459925.
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    8. Wang L, Stevens KA, Haupt-Renaud P, Marcus RK. Dynamic evaluation of a trilobal capillary-channeled polymer fiber shape for reversed phase protein separations and comparison to the eight-channeled form. J Sep Sci. 2018 Mar; 41(5):1063-1073. PMID: 29232068.
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    9. Hoegg ED, Marcus RK, Koppenaal DW, Irvahn J, Hager GJ, Hart GL. Determination of uranium isotope ratios using a liquid sampling atmospheric pressure glow discharge/Orbitrap mass spectrometer system. Rapid Commun Mass Spectrom. 2017 Sep 30; 31(18):1534-1540. PMID: 28696545.
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    10. Jiang L, Marcus RK. Microwave-assisted, grafting polymerization preparation of strong cation exchange nylon 6 capillary-channeled polymer fibers and their chromatographic properties. Anal Chim Acta. 2017 Jul 18; 977:52-64. PMID: 28577598.
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    11. Trang HK, Marcus RK. Application of protein A-modified capillary-channeled polymer polypropylene fibers to the quantitation of IgG in complex matrices. J Pharm Biomed Anal. 2017 Aug 05; 142:49-58. PMID: 28494339.
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    12. Jiang L, Marcus RK. Microwave-assisted grafting polymerization modification of nylon 6 capillary-channeled polymer fibers for enhanced weak cation exchange protein separations. Anal Chim Acta. 2017 Feb 15; 954:129-139. PMID: 28081807.
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    13. Haupt-Renaud P, Jiang L, Marcus RK. Preliminary assessment of the modification of polystyrene-divinylbenzene resin with lipid-tethered ligands for selective separations. J Sep Sci. 2016 Oct; 39(20):3868-3879. PMID: 27541805.
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    14. Marcus RK, Paing HW, Zhang LX. Conceptual Demonstration of Ambient Desorption-Optical Emission Spectroscopy Using a Liquid Sampling-Atmospheric Pressure Glow Discharge Microplasma Source. Anal Chem. 2016 06 07; 88(11):5579-84. PMID: 27175512.
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    15. Hoegg ED, Barinaga CJ, Hager GJ, Hart GL, Koppenaal DW, Marcus RK. Preliminary Figures of Merit for Isotope Ratio Measurements: The Liquid Sampling-Atmospheric Pressure Glow Discharge Microplasma Ionization Source Coupled to an Orbitrap Mass Analyzer. J Am Soc Mass Spectrom. 2016 08; 27(8):1393-403. PMID: 27080006.
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    16. Trang HK, Schadock-Hewitt AJ, Jiang L, Marcus RK. Evaluation of loading characteristics and IgG binding performance of Staphylococcal protein A on polypropylene capillary-channeled polymer fibers. J Chromatogr B Analyt Technol Biomed Life Sci. 2016 Mar 15; 1015-1016:92-104. PMID: 26919444.
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    17. Marcus RK, Baeumner AJ. Fiber-based platforms for bioanalytics. Anal Bioanal Chem. 2016 Feb; 408(5):1281-3. PMID: 26715245.
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    18. Zhang LX, Jiang L, Willett DR, Marcus RK. Parallel, open-channel lateral flow (immuno) assay substrate based on capillary-channeled polymer films. Analyst. 2016 Feb 07; 141(3):807-14. PMID: 26646022.
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    19. Zhang LX, Burdette CQ, Phillips MM, Rimmer CA, Marcus RK. Determination of Isoflavone Content in SRM 3238 Using Liquid Chromatography-Particle Beam/Electron Ionization Mass Spectrometry. J AOAC Int. 2015 Nov-Dec; 98(6):1483-90. PMID: 26651559.
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    20. Schadock-Hewitt AJ, Bruce TF, Marcus RK. Evidence for the Intercalation of Lipid Acyl Chains into Polypropylene Fiber Matrices. Langmuir. 2015 Sep 29; 31(38):10418-25. PMID: 26381380.
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    21. Jiang L, Marcus RK. Comparison of analytical protein separation characteristics for three amine-based capillary-channeled polymer (C-CP) stationary phases. Anal Bioanal Chem. 2016 Feb; 408(5):1373-83. PMID: 26345444.
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    22. Jiang L, Jin Y, Marcus RK. Polyethylenimine modified poly(ethylene terephthalate) capillary channeled-polymer fibers for anion exchange chromatography of proteins. J Chromatogr A. 2015 Sep 04; 1410:200-9. PMID: 26253835.
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    23. Zhang LX, Manard BT, Powell BA, Marcus RK. Preliminary Assessment of Potential for Metal-Ligand Speciation in Aqueous Solution via the Liquid Sampling-Atmospheric Pressure Glow Discharge (LS-APGD) Ionization Source: Uranyl Acetate. Anal Chem. 2015 Jul 21; 87(14):7218-25. PMID: 26134783.
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    24. Manard BT, Jones SM, Marcus RK. Capillary-channeled polymer (C-CP) fibers for the rapid extraction of proteins from urine matrices prior to detection with MALDI-MS. Proteomics Clin Appl. 2015 Jun; 9(5-6):522-30. PMID: 25450308.
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    25. Jiang L, Schadock-Hewitt AJ, Zhang LX, Marcus RK. Evaluation of synthesized lipid tethered ligands for surface functionalization of polypropylene capillary-channeled polymer fiber stationary phases. Analyst. 2015 Mar 07; 140(5):1523-34. PMID: 25619845.
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    26. Manard BT, Konegger-Kappel S, Gonzalez JJ, Chirinos J, Dong M, Mao X, Marcus RK, Russo RE. Liquid sampling-atmospheric pressure glow discharge as a secondary excitation source for laser ablation-generated aerosols: parametric dependence and robustness to particle loading. Appl Spectrosc. 2015 Jan; 69(1):58-66. PMID: 25506884.
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    27. Jiang L, Marcus RK. Biotin-functionalized poly(ethylene terephthalate) capillary-channeled polymer fibers as HPLC stationary phase for affinity chromatography. Anal Bioanal Chem. 2015 Jan; 407(3):939-51. PMID: 25410640.
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    28. Wang Z, Marcus RK. Roles of interstitial fraction and load conditions on the dynamic binding capacity of proteins on capillary-channeled polymer fiber columns. Biotechnol Prog. 2015 Jan-Feb; 31(1):97-109. PMID: 25378292.
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    29. Schadock-Hewitt AJ, Marcus RK. Loading characteristics and chemical stability of headgroup-functionalized poly(ethylene glycol)-lipid ligand tethers on polypropylene capillary-channeled polymer fibers. J Sep Sci. 2014 Dec; 37(24):3595-602. PMID: 25284707.
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    30. Zhang LX, Manard BT, Konegger-Kappel S, Kappel SK, Marcus RK. Evaluation of the operating parameters of the liquid sampling-atmospheric pressure glow discharge (LS-APGD) ionization source for elemental mass spectrometry. Anal Bioanal Chem. 2014 Nov; 406(29):7497-509. PMID: 25002336.
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    31. Wang Z, Marcus RK. Determination of pore size distributions in capillary-channeled polymer fiber stationary phases by inverse size-exclusion chromatography and implications for fast protein separations. J Chromatogr A. 2014 Jul 18; 1351:82-9. PMID: 24877979.
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    32. Schadock-Hewitt AJ, Pittman JJ, Christensen KA, Marcus RK. Head group-functionalized poly(ethyleneglycol)-lipid (PEG-lipid) surface modification for highly selective analyte extractions on capillary-channeled polymer (C-CP) fibers. Analyst. 2014 May 07; 139(9):2108-13. PMID: 24503581.
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    33. Schadock-Hewitt AJ, Marcus RK. Initial evaluation of protein A modified capillary-channeled polymer fibers for the capture and recovery of immunoglobulin G. J Sep Sci. 2014 Mar; 37(5):495-504. PMID: 24376153.
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    34. Burdette CQ, Marcus RK. Determination of isoflavone content in soy, red clover, and kudzu dietary supplement materials by liquid chromatography-particle beam/electron ionization mass spectrometry. J AOAC Int. 2013 Sep-Oct; 96(5):925-32. PMID: 24282927.
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    35. Marcus RK, Burdette CQ, Manard BT, Zhang LX. Ambient desorption/ionization mass spectrometry using a liquid sampling-atmospheric glow discharge (LS-APGD) ionization source. Anal Bioanal Chem. 2013 Oct; 405(25):8171-84. PMID: 23877182.
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    36. Randunu KM, Marcus RK. Initial evaluation of protein throughput and yield characteristics on nylon 6 capillary-channeled polymer (C-CP) fiber stationary phases by frontal analysis. Biotechnol Prog. 2013 Sep-Oct; 29(5):1222-9. PMID: 23804494.
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    37. Kole C, Kole P, Randunu KM, Choudhary P, Podila R, Ke PC, Rao AM, Marcus RK. Nanobiotechnology can boost crop production and quality: first evidence from increased plant biomass, fruit yield and phytomedicine content in bitter melon (Momordica charantia). BMC Biotechnol. 2013 Apr 26; 13:37. PMID: 23622112.
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    38. Burdette CQ, Marcus RK. In-line desalting of proteins from buffer and synthetic urine solution prior to ESI-MS analysis via a capillary-channeled polymer fiber microcolumn. J Am Soc Mass Spectrom. 2013 Jun; 24(6):975-8. PMID: 23463546.
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    39. Burdette CQ, Marcus RK. Solid phase extraction of proteins from buffer solutions employing capillary-channeled polymer (C-CP) fibers as the stationary phase. Analyst. 2013 Feb 21; 138(4):1098-106. PMID: 23223274.
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    40. Randunu KM, Dimartino S, Marcus RK. Dynamic evaluation of polypropylene capillary-channeled fibers as a stationary phase in high-performance liquid chromatography. J Sep Sci. 2012 Dec; 35(23):3270-80. PMID: 23109248.
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    41. Randunu KM, Marcus RK. Microbore polypropylene capillary channeled polymer (C-CP) fiber columns for rapid reversed-phase HPLC of proteins. Anal Bioanal Chem. 2012 Aug; 404(3):721-9. PMID: 22736228.
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    42. Manard BT, Marcus RK. Capillary-channeled polymer (C-CP) fibers as a stationary phase for sample clean-up of protein solutions for matrix-assisted laser/desorption ionization mass spectrometry. J Am Soc Mass Spectrom. 2012 Aug; 23(8):1419-23. PMID: 22653465.
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    43. Pittman JJ, Manard BT, Kowalski PJ, Marcus RK. Capillary-channeled polymer (C-CP) films as processing platforms for protein analysis by matrix-assisted laser/desorption ionization mass spectrometry (MALDI-MS). J Am Soc Mass Spectrom. 2012 Jan; 23(1):102-7. PMID: 22012690.
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    44. Quarles CD, Carado AJ, Barinaga CJ, Koppenaal DW, Marcus RK. Liquid sampling-atmospheric pressure glow discharge (LS-APGD) ionization source for elemental mass spectrometry: preliminary parametric evaluation and figures of merit. Anal Bioanal Chem. 2012 Jan; 402(1):261-8. PMID: 21910014.
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    45. Quarles CD, Randunu KM, Brumaghim JL, Marcus RK. Metal retention in human transferrin: consequences of solvent composition in analytical sample preparation methods. Metallomics. 2011 Oct; 3(10):1027-34. PMID: 21904748.
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    46. Winn B, Quarles CD, Marcus RK, LaBerge M. Nickel ions inhibit a-actin expression and decrease aspect ratio of rat vascular smooth muscle cells in vitro. Metallomics. 2011 Sep; 3(9):934-40. PMID: 21766118.
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    47. Quarles CD, Marcus RK, Brumaghim JL. Competitive binding of Fe3+, Cr3+, and Ni2+ to transferrin. J Biol Inorg Chem. 2011 Aug; 16(6):913-21. PMID: 21678080.
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    48. Quarles CD, Brumaghim JL, Marcus RK. Instrumental comparison of the determination of Cr³+ uptake by human transferrin. Metallomics. 2010 Dec; 2(12):792-9. PMID: 21510013.
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    49. Castro J, Krishna MV, Marcus RK. Liquid chromatography-particle beam electron ionization mass spectrometry method for analysis of botanical extracts: evaluation of ephedrine alkaloids in standard reference materials. J AOAC Int. 2010 Nov-Dec; 93(6):1788-97. PMID: 21313804.
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    50. Hilbert KJ, Marcus RK. Separation of water-soluble polymers using capillary-channeled polymer fiber stationary phases. J Sep Sci. 2010 Nov; 33(22):3571-7. PMID: 20972973.
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    51. Castro J, Pregibon T, Chumanov K, Marcus RK. Determination of catechins and caffeine in proposed green tea standard reference materials by liquid chromatography-particle beam/electron ionization mass spectrometry (LC-PB/EIMS). Talanta. 2010 Oct 15; 82(5):1687-95. PMID: 20875564.
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    52. Castro J, Krishna MV, Choiniere JR, Marcus RK. Analysis of caffeic acid derivatives in echinacea extracts by liquid chromatography particle beam mass spectrometry (LC-PB/MS) employing electron impact and glow discharge ionization sources. Anal Bioanal Chem. 2010 Jun; 397(3):1259-71. PMID: 20349350.
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    53. Straut CM, Marcus RK. Small molecule adsorption on to polyester capillary-channeled polymer fibers: frontal analysis of naphthalene and naphthol (naphthalene and naphthol adsorption on capillary-channeled polymer fibers). J Sep Sci. 2010 Jan; 33(1):46-60. PMID: 20091715.
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    54. Quarles CD, Brumaghim JL, Marcus RK. Simultaneous multiple element detection by particle beam/hollow cathode-optical emission spectroscopy as a tool for metallomic studies: determinations of metal binding with apo-transferrin. Metallomics. 2010 Feb; 2(2):154-61. PMID: 21069147.
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    55. Marcus RK. Use of polymer fiber stationary phases for liquid chromatography separations: part II--Applications. J Sep Sci. 2009 Mar; 32(5-6):695-705. PMID: 19194974.
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    56. Stanelle RD, Marcus RK. Nylon-6 capillary-channeled polymer (C-CP) fibers as a hydrophobic interaction chromatography stationary phase for the separation of proteins. Anal Bioanal Chem. 2009 Jan; 393(1):273-81. PMID: 18958449.
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    57. Marcus RK. Use of polymer fiber stationary phases for liquid chromatography separations: Part I--Physical and chemical rationale. J Sep Sci. 2008 Jun; 31(11):1923-35. PMID: 18615816.
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    58. Stanelle RD, Straut CM, Marcus RK. Nylon-6 capillary-channeled polymer fibers as a stationary phase for the mixed-mode ion exchange/reversed-phase chromatography separation of proteins. J Chromatogr Sci. 2007 Aug; 45(7):415-21. PMID: 17725868.
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    59. Brewer TM, Marcus RK. Separation and determination of iron-containing proteins via liquid chromatography-particle beam/hollow cathode-optical emission spectroscopy. Anal Chem. 2007 Mar 15; 79(6):2402-11. PMID: 17298030.
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    60. Nelson DM, Marcus RK. Characterization of capillary-channeled polymer fiber stationary phases for high-performance liquid chromatography protein separations: Comparative analysis with a packed-bed column. Anal Chem. 2006 Dec 15; 78(24):8462-71. PMID: 17165840.
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    61. Venzie JL, Castro J, Balarama Krishna MV, Nelson DM, Marcus RK. Electron-impact and glow-discharge ionization LC-MS analysis of green tea tincture. Anal Bioanal Chem. 2007 Jan; 387(1):321-33. PMID: 17139484.
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    62. Brewer TM, Marcus RK. Non-metal element detection by radio-frequency glow-discharge optical-emission spectrometry (rf-GD-OES) for determination of sol-gel-immobilized nucleotides. Anal Bioanal Chem. 2006 Nov; 386(5):1357-65. PMID: 16906385.
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    63. Fornea DS, Wu Y, Marcus RK. Capillary-channeled polymer fibers as a stationary phase for desalting of protein solutions for electrospray ionization mass spectrometry analysis. Anal Chem. 2006 Aug 01; 78(15):5617-21. PMID: 16878906.
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    64. Nelson DM, Marcus RK. Potential for ultrafast protein separations with capillary-channeled polymer (C-CP) fiber columns. Protein Pept Lett. 2006; 13(1):95-9. PMID: 16454677.
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    65. Stanelle RD, Mignanelli M, Brown P, Marcus RK. Capillary-channeled polymer (C-CP) fibers as a stationary phase in microbore high-performance liquid chromatography columns. Anal Bioanal Chem. 2006 Jan; 384(1):250-8. PMID: 16283270.
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    66. Stanelle RD, Sander LC, Marcus RK. Hydrodynamic flow in capillary-channel fiber columns for liquid chromatography. J Chromatogr A. 2005 Dec 23; 1100(1):68-75. PMID: 16194542.
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    67. Venzie JL, Marcus RK. Micro-scale analytical plasmas for liquid chromatography detection. Anal Bioanal Chem. 2005 Jan; 381(1):96-8. PMID: 15599714.
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    68. Jin F, Hickman JJ, Lenghaus K, Marcus RK. Total protein determinations by particle beam/hollow cathode optical emission spectroscopy (PB/HC-OES) system III: investigation of carrier salts for enhanced particle transport. Anal Bioanal Chem. 2004 Sep; 380(2):204-11. PMID: 15278336.
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    69. Nelson DK, Marcus RK. A novel stationary phase: capillary-channeled polymer (C-CP) fibers for HPLC separations of proteins. J Chromatogr Sci. 2003 Oct; 41(9):475-9. PMID: 14596784.
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    70. Jin F, Lenghaus K, Hickman J, Marcus RK. Total protein determinations by particle beam/hollow cathode optical emission spectroscopy. Anal Chem. 2003 Sep 15; 75(18):4801-10. PMID: 14674457.
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    71. Davis WC, Knippel BC, Cooper JE, Spraul BK, Rice JK, Smith DW, Marcus RK. Use of sol-gels as solid matrixes for simultaneous multielement determination by radio frequency glow discharge optical emission spectrometry: determinations of suspended particulate matter. Anal Chem. 2003 May 15; 75(10):2243-50. PMID: 12918962.
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    72. Marcus RK, Davis WC, Knippel BC, LaMotte L, Hill TA, Perahia D, Jenkins JD. Capillary-channeled polymer fibers as stationary phases in liquid chromatography separations. J Chromatogr A. 2003 Jan 31; 986(1):17-31. PMID: 12585319.
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    73. Davis WC, Venzie JL, Willis B, Coffee RL, Arya DP, Marcus RK. Particle beam glow discharge mass spectrometry: spectral characteristics of nucleobases. Rapid Commun Mass Spectrom. 2003; 17(15):1749-58. PMID: 12872280.
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    74. Marcus RK, Anfone AB, Luesaiwong W, Hill TA, Perahia D, Shimizu K. Radio frequency glow discharge optical emission spectroscopy: a new weapon in the depth profiling arsenal. Anal Bioanal Chem. 2002 Aug; 373(7):656-63. PMID: 12185579.
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    75. Marcus RK, Davis WC. An atmospheric pressure glow discharge optical emission source for the direct sampling of liquid media. Anal Chem. 2001 Jul 01; 73(13):2903-10. PMID: 11467534.
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    76. Gibeau TE, Marcus RK. Separation and identification of organic and organometallic compounds by use of a liquid chromatography-particle beam-glow discharge mass spectrometry combination. J Chromatogr A. 2001 Apr 27; 915(1-2):117-28. PMID: 11358240.
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    77. Marcus RK, Dempster MA, Gibeau TE, Reynolds EM. Sampling and analysis of particulate matter by glow discharge atomic emission and mass spectrometries. Anal Chem. 1999 Aug 01; 71(15):3061-9. PMID: 21662898.
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    78. You J, Dempster MA, Marcus RK. Analysis of organic compounds by particle beam/hollow cathode atomic emission spectroscopy:? determinations of carbon and hydrogen in amino acids. Anal Chem. 1997 Sep 01; 69(17):3419-26. PMID: 21639264.
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    79. Parker M, Hartenstein ML, Marcus RK. Influence of discharge parameters on the resultant sputtered crater shapes for a radio frequency glow discharge atomic emission source. Anal Chem. 1996 Dec 01; 68(23):4213-20. PMID: 21619332.
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    80. Shick CR, Depalma PA, Marcus RK. Radio frequency glow discharge mass spectrometry for the characterization of bulk polymers. Anal Chem. 1996 Jul 01; 68(13):2113-21. PMID: 21619297.
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    81. Cable PR, Parker M, Marcus RK, Pochkowski JM. Direct generation of ion beam images with a two-dimensional charge injection device. J Am Soc Mass Spectrom. 1995 Feb; 6(2):140-7. PMID: 24222076.
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    82. Discharge G, Mei Y, Duckworth DC, Cable PR, Marcus RK. Effects of target gas in collision-induced dissociation using a double quadrupole mass spectrometer and radiofrequency. J Am Soc Mass Spectrom. 1994 Sep; 5(9):845-51. PMID: 24222032.
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    83. Winchester MR, Marcus RK. Emission characteristics of a pulsed, radiofrequency glow discharge atomic emission device. Anal Chem. 1992 Sep; 64(18):2067-74. PMID: 19518040.
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